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Using the Transient Plane Source Method for Measuring Thermal Parameters of Electroceramics

Authors: Peter Krupa, Svetozár Malinarič


Transient plane source method has been used to measure the thermal diffusivity and thermal conductivity of a compact isostatic electroceramics at room temperature. The samples were fired at temperatures from 100 up to 1320 degrees Celsius in steps of 50. Bulk density and specific heat capacity were also measured with their corresponding standard uncertainties. The results were compared with further thermal analysis (dilatometry and thermogravimetry). Structural processes during firing were discussed.

Keywords: TPS method, thermal conductivity, thermal diffusivity, thermal analysis, electroceramics, firing.

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[1] C. Y. Chen, G. S. Lan and W. H. Tuan, "Microstructural evolution of mullite during the sintering of kaolin powder compacts”, Ceramics International, Elsevier, vol. 26, pp. 715–720, 2000
[2] M. Benea and M. Gorea, "Mineralogy and technological properties of some kaolin types used in the ceramic industry”, Studia Universitatis Babes¸-Bolyai, Geologia, vol. XLIX, pp. 33–39, 2004
[3] H. Wang, Ch. Li, Z. Peng and S. Zhang, "Characterization and thermal behavior of kaolin”, Journal of Thermal Analysis and Calorimetry, Springer, vol. 105, pp. 157–160, 2011
[4] M. S. Karmous, "Theoretical study of kaolinite structure; energy minimization and crystal properties”, World Journal of Nano Science and Engineering, Scientific Research, vol. 1, pp. 62–66, 2011
[5] T. Hu´lan, A. Trnı´k, I. Sˇ tubnˇa and I. Medved’, "Thermal and elastic properties of kaolin Sedlec”, Thermophysics 2013, 18th International Meeting of Thermophysical Society – Conference Proceedings, Brno University of Technology, pp. 40–46, 2013
[6] S. E. Gustaffson, "Transient plane source techniques for thermal conductivity and thermal diffusivity measurements of solid materials”, Review of Scientific Instruments, vol. 62, pp. 797–804, 1991.
[7] M. K. Gustavsson, E. Karawacki and S. E. Gustafsson, "Thermal conductivity, thermal diffusivity and specific heat of thin samples from transient measurements with hot-disk sensors”, Review of Scientific Instruments, vol. 65, pp. 3856–3859, 1994.
[8] M. M. Suleiman, S. E. Gustafsson and L. Bo¨rjesson, "A practical cryogenic resistive sensor for thermal conductivity measurements”, Sensors and Actuactors, vol. 57, 1996
[9] V. Boha´cˇ, M. K. Gustavsson, L’. Kubicˇa´r, S. E. Gustafsson, "Parameter estimations for measurements of thermal transport properties with the hot disk thermal constants analyzer”, Review of Scientific Instruments, Elsevier, vol. 71, pp. 15–19, 2000
[10] M. K. Gustavsson, S. E. Gustafsson, "On power variation in self-heated thermal sensors”, Thermal Conductivity 27, DEStech Publications, Inc., vol. 27, pp. 338–346, 2003.
[11] ISO 22007-2, "Plastics — Determination of thermal conductivity and thermal diffusivty — Transient plane heat source (hot disc) method”, Geneva, 2008
[12] P. Johansson, B. Adl-Zarrabi, C. Hagentoft, "Usint transient plane source sensor for determination of thermal properties of vacuum insulation panels”, Frontiers of Architectural Research, Higher Education Press, vol. 1, pp. 334–340, 2012.
[13] R. Coquard, E. Coment, G. Flasquin and D. Baillis, "Analysis of the hot-disk technique applied to low-density insulating materials”, International Journal of Thermal Sciences, Elsevier, vol. 65, pp. 242–253, 2013.
[14] Y. Li, Ch. Shi, J. Liu, E. Liu, J. Shao, Z. Chen, D. J. Dorantes-Gonzales and X. Hu, "Improving the accuracy of the transient plane source method by correcting probe heat capacity and resistance influences”, Measurement Science and Technology, IOP Publishing Ltd, vol. 25, 2014
[15] S. Malinaricˇ and P. Diesˇka, "Dynamic measurements of the temperature coefficient of resistance in the transient plane source method”, Int. Journal of Thermophysics, Springer, vol. 30, pp. 1557–1567, 2009
[16] S. Malinaricˇ, "Contribution to the transient plane source method for measuring thermophysical properties of solids”, International Journal of Thermophysics, Springer, vol. 34, pp. 1953–1961, 2013
[17] P. Pytlı´k and R. Sokola´rˇ, Stavebnı´ keramika – technologie, vlastnosti a vyuzˇitı´, Akademicke´ nakladatelstvı´ CERM, s.r.o., Brno, 2002