Search results for: halogenation
2 Technologies of Halogenation of Hydroxyanthraquinones
Authors: Dmitriy Yu. Korulkin, Raissa A. Muzychkina
Abstract:
In review the generalized data about different methods of synthesis of biological activity halogenated di-, tri- and tetrahydroxyanthraquinones is presented. The basic regularity of a synthesis is analyzed. Action of temperature, pH, solubility, catalysts and other factors on a reaction product yield is revealed.
Keywords: Electrophilic substitution, halogenation, hydroxyanthraquinones, physiologically active substances.
Procedia APA BibTeX Chicago EndNote Harvard JSON MLA RIS XML ISO 690 PDF Downloads 21431 Improvement of Reaction Technology of Decalin Halogenation
Authors: Dmitriy Yu. Korulkin, Ravshan M. Nuraliev, Raissa A. Muzychkina
Abstract:
In this research paper were investigated the main regularities of a radical bromination reaction of decalin. There had been studied the temperature effect, durations of reaction, frequency rate of process, a ratio of initial components, type and number of the initiator on decalin bromination degree. There were specified optimum conditions of synthesis of a perbromodecalin by the method of a decalin bromination. There are developed the technological flowchart of receiving a perbromodecalin and the mass balance of process on the first and the subsequent loadings of components. The results of research of antibacterial and antifungal activity of synthesized bromoderivatives have been represented.
Keywords: Decalin, optimum technology, perbromodecalin, radical bromination.
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