%0 Journal Article %A I. Grigoraviciute-Puroniene and K. Tsuru and E. Garskaite and Z. Stankeviciute and A. Beganskiene and K. Ishikawa and A. Kareiva %D 2017 %J International Journal of Chemical and Molecular Engineering %B World Academy of Science, Engineering and Technology %I Open Science Index 124, 2017 %T Wet Polymeric Precipitation Synthesis for Monophasic Tricalcium Phosphate %U https://publications.waset.org/pdf/10006847 %V 124 %X Tricalcium phosphate (β-Ca3(PO4)2, β-TCP) powders were synthesized using wet polymeric precipitation method for the first time to our best knowledge. The results of X-ray diffraction analysis showed the formation of almost single a Ca-deficient hydroxyapatite (CDHA) phase of a poor crystallinity already at room temperature. With continuously increasing the calcination temperature up to 800 °C, the crystalline β-TCP was obtained as the main phase. It was demonstrated that infrared spectroscopy is very effective method to characterize the formation of β-TCP. The SEM results showed that β-TCP solids were homogeneous having a small particle size distribution. The β-TCP powders consisted of spherical particles varying in size from 100 to 300 nm. Fabricated β-TCP specimens were placed to the bones of the rats and maintained for 1-2 months. %P 320 - 323